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Peptides were eluted using a linear gradient of H 2 O:CH 3 CN (98:2, 0.1% formic acid) to H 2 O:CH 3 CN (64:36, 0.1% formic acid) at 200 L/min over 30 min

So I really have to find a source, again, another source, then to clean up my raw materials, completely give me metal free